Pure methamphetamine should begin crystallization between 170˚C and 175˚C, and with cut methamphetamine this would happen at a lower temperature. New comments cannot be posted and votes cannot be cast. General was happily smoking a few bowls in his office in no time. A reliable heating device like an oven could be used to remove some MSM in theory (250 degrees F off the top of my head, but don’t quote me on that). tl;dr: the best tests for n-iso cuts are melting point test, and by qualitative analysis of crystallization patterns. N-iso takes forever to evaporate, and when it does, there will be a geometric-looking crystal left behind, that's wet in the middle when you crush it. Will this kinda thermometer work ? The crystals are beautiful and translucent. Just straight bleach. The vapor will also be somewhat cool feeling, like a hint of menthol. The free base seemed easiest, and can be used as-is, so I figured I should go that route to start with, but it's by no means settled yet. The upper layer will be entirely liquid. Heat it until it starts to melt, and they'll react, producing an upper layer of n-iso and meth, and a lower layer of water, KCl and KOH. I'm not sure that simple evaporation is the best way to separate them, although it is the smallest number of steps, and has been proven to reduce the n-iso fraction considerably. Is there anything bad about ingesting n-iso, I mean, more so than large amounts of meth? A much more sinister cut is that of isopropylbenzylamine. DEA chemists coordinated worldwide LE by going through the hundreds of compounds matching up the reagent results, appearance, melting point probably taste to arrive at n-iso. MDL number MFCD00008863. Out. You will want to use he original type of Clorox bleach that doesn’t have an additives or fragrances added it it. Since you're not a chemist, don't fuck around with it to try and speed things up. I've been trying to educate people on this for a while, just because until people learn to spot fake shit, we're gonna keep getting it on a regular basis like this. If I had as much as you do though, the way I'd separate them would be with ion-exchange chromatography. Molecular Weight 149.23 . Pure methamphetamine “cracksback” after it is liquefied by heat. Fuck n-isopropylbenzylamine. So, how do you test it? The quality is top notch, melting point analysis showed absolutely no residue. I also can't really say if would even work at that scale. No MSM is present in this methamphetamine (it sublimates around 250 degrees, while methamphetamine has a higher vaporization temperature). In my personal experience though they sell straight bunk or straight good shit. Yes, sodium hydroxide can also work, but not as well, and you'll lose more, so if you can afford methamphetamine, you can afford potassium hydroxide. Quote: ^^^ Go to the head of the class. It cocrystallizes with methamphetamine and has an identical weight. What was i fucking smoking? bmw e46 transmission fault code 59 pdfsdocuments2 pdf&id=d41d8cd98f00b204e9800998ecf8427e book review, free download Ouch... You have clicked a page that seems to be very popular. View information & documentation regarding N -Isopropylbenzylamine, including CAS, MSDS & more. Well, it's very, very difficult to separate them, which is the whole reason this bullshit became popular for cutting. If you're in a hurry and don't want to wait overnight, or however long it takes n-iso to dry, you can dissolve it in at least 90% isopropanol rubbing alcohol instead of water. The crystals break down just as pure methamphetamine should as MSM (Methylsulfonylmethane) and isopropylbenzylamine noticeably change how brittle they are. You cant even get a decent answer for what meth and other cuts are soluble in what solvents. The pattern looks like bird feathers. If you're not a chemist, you can separate them based on the fact that the freebase of n-iso evaporates more easily. I checked this up because as luck would have it SWIM in North Korea superlab was doing a dual solvent recrystalization on a batch he had fuckedup and mixed it into n-iso. (where are those guys? N-iso is not soluble in acetone, however a dual-solvent crystallization can do some good to separate them. This is great stuff right here man, it just seems like a lot of work for the typical instant gratification drug user. It's the inevitable result of tweakers using crystal size and clarity as a way of measuring purity. KOH is also less corrosive to glass, despite being a stronger base. Severe cases result in comas, seizures, and death. Anyway, after having taken a proper kicking from the generals black shiny marching boots, had to fix it pronto. If a shard of methamphetamine placed in the bleach solution releases an oil, a cut is present although it is not possible to pinpoint the exact one. They are relatively clear and are not cloudy. Ok, so after about an hour of searching i found the answer, N-ISO IS SOLUBLE IN ACETONE. It's probably not especially harmful, it's just that some of the stuff that's out there can be cut such that there's only 10-15% methamphetamine, and the rest all n-iso. Its not, all same fucking shit n-iso flat shards. One thing I learned is that this cut happened in Mexico, so the downstream sellers don't necessarily know that what they're selling is shit. Dont believe half of what you read. If a darknet vendor is advertising the size and clarity of their crystals, rest assured, that shit is faker than a 40-year-old stripper's boobs. Discover the magic of the internet at Imgur, a community powered entertainment destination. The general, who is prone for a bit of sampling the new batches they turn out, got a real big lungful of n-iso. If you don't have enough for a melting point test, dissolve as much as possible in a small amount of distilled water, then put a few drops on a smooth flat surface, like a mirror or a plate. NaOH doesn't produce as good of a separation, meaning you have to do multiple extractions, which leads to high mechanical losses if you're not starting with much. I actually have a lot of random attempts at research like that. This has been happening since about February 2017. Put mineral oil or cooking oil or some other clear liquid with a high boiling point in the beaker, then put the test tube in that and heat it on a stove burner or a flame or something. Get a test tube or a narrow vial or something, put a bunch of your shit in it, then put some potassium hydroxide flakes on top. What kind of thermometer? This can be done in a chromatography column with polystyrene sulfonate ion exchange resin. N-Isopropylbenzylamine 97% Synonym: N-Benzylisopropylamine CAS Number 102-97-6. EC Number 203-067-6. So just let it sit at room temperature until the physical properties resemble methamphetamine more than n-iso. Looking at your history, I see you have quite a lot of this stuff. These two substances only have similar properties in the form of their hydrochloride salts though, and are less similar in other forms. Bleach can be used as an indicator to hint at the presence of the compound. Lift your spirits with funny jokes, trending memes, entertaining gifs, inspiring stories, viral videos, and so much more. Background. Theres one guy whos got multiple listings on all the sites, "Top+++ methampetamine: the best" all made to look like diff listings. Symptoms include shortness of breath, discolored skin, headaches, fatigue, and loss of consciousness. Definitely try at a small scale first. Come back mid 2017 and its all fucking garbage. Anyone can hook me up with an email or wikr you would be my BFF.) Okay, so it's cut, now what? Compounds related to isopropylbenzylamine are also used as cutting agents such as methylbenzylamine and ethylbenzylamine. Eventually, the stuff in the tube will melt, and when it does, insert the thermometer. Nothing is perfect though and on this site I saw suspicious posts looking like LE distributing disinformation, namely that n-iso was not soluble in acetone and more bullshit about meth. (the last one is sorta like crackback but more scientific) if you need to separate them, the free bases are easier to separate than the HCl salts. There is so much fucking FUD on the web, on redditt and on others like blulight. As soon as it starts to form crystals, make a note of the temperature. thank you. One thing I learned is that this cut happened in Mexico, so the downstream sellers don't necessarily know that what they're selling is shit. There are some parts I'm less sure of than others, but one thing that I think is new here is using KOH instead of NaOH for getting the free base. Bleach can be used as an indicator to hint at the presence of the compound. You can get it used for not much.
I never had enough for testing that I could have a good estimate of yields though. The melting point test is for distinguishing a mixture from a pure substance. Probably 0%. I want to set up a group #deathtoallscammers and #scammersmustdie. You can have a rest and please slide to verify. Then just recrystallize that once or twice to get rid of the excess HCl. Sigma-Aldrich offers a number of N -Isopropylbenzylamine products. Its not!! The CLP Regulation ensures that the hazards presented by chemicals are clearly communicated to workers and consumers in the European Union through classification and labelling of … Some people prefer the freebase, but if you prefer the HCl salt, then figure out how to get it yourself. As a warning, isopropylbenzylamine ingested regularly over time will cause methmoglobinemia. Mixtures experience melting point depression, and a wide melting point range, unlike pure substances. How to make isopropylbenzylamine How to make isopropylbenzylamine When the heat source is removed, the puddle recrystallizes with an audible cracking sound. Linear Formula C 6 H 5 CH 2 NHCH(CH 3) 2. If it's highly-cut, then this number will be about ten degrees lower by the time it's fully solid. Who do you think came up with the idea? Take a shot glass and fill it with bleach. dual solvent recrystalization with acetone first then iopropyl alcohol second. This really pissed me off cos I was looking here on removing n-iso. This has been happening since about February 2017. The simplest method I listed can really only concentrate it, and is subject to losses. If it's pure, this temperature should not change much at all during solidification. If it does, that means that you now have a mixture and not a pure substance, since the two substances weren't identical. For anyone unfamiliar, Mexican cartels have been heavily cutting the meth they make before smuggling it into the US. amazing post. This methamphetamine cracks back instantly, failure to crackback or a large delay indicates impure product.
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